WP-TEC-1020PLC Low-Temperature Pressurized Photocatalytic Reactor

Basic Parameters

Reaction Sites: 10 groups (The 11th is a blank temperature measurement point)

Reaction Vessel: 20mL (Round bottom, small tube diameter, thick wall, glass reaction tube)

Applicable Volume: 1-5mL (Sealed tube, lighting), 1-10mL (Room temperature, heating, lighting)

Applicable Reactions: Stirring reaction, heating reaction, sealed tube reaction, anhydrous and oxygen-free reaction

High-Temperature Parameters:

Heating Unit: Intelligent Safety Heater (equipped with German IKA heater)

Temperature Control Unit: Precision Intelligent Probe (equipped with German IKA precision probe)

Temperature Control Technology: Internal temperature control + Parallel temperature control + Electronic dual temperature control

Independent Temperature Zone: 1 temperature control zone (Heating module is standard)

Heating Range: RT-220℃ ☆

Heating Efficiency: 5-8℃/min (10 units of 5mL ethanol, 20-100℃)

Sealed Tube Experiment: Yes (True sealed tube, zero reflux sealed tube)

Overnight Experiment: Yes (Overnight temperature ≤120℃)

Cooling and Temperature Reduction: Yes (Requires external cooling circulation, panel-integrated float water flow meter)

Reflux Parameters: If "Reflux Module" is selected (not configured)

Reflux Experiment: Standard condenser reflux module (enables photocatalysis under reflux)

Reflux Experiment: Yes (Reflux efficiency ≥98%, ethanol loss rate ≤2% after 48h heating reflux at 80℃)

Low-Temperature Parameters: If "Low-Temperature Module" is selected (configured)

Low-Temperature Experiment: Standard low-temperature module (does not include low-temperature circulation pump)

Cooling Method: Can be connected to an external circulation chiller

Low-Temperature Range: Can reach as low as -20℃ (depending on the external circulation chiller)

Temperature Control Difference: ±1℃ (depending on the self-provided external circulation chiller)

Pressure Parameters: If "Pressure Function" is selected (configured)

Gas Addition Experiment: Standard pressure-resistant components (enables photocatalytic reaction under low pressure)

Gas Addition Method: Gas supplied to the system via pipeline from gas cylinder connected to the gas source platform

Pressure Range: Maximum gas pressure up to 10atm

Pressure Display: Adjust charging pressure range via pressure gauge at the outlet of the pressure reducer

Photocatalytic Parameters: If "Lighting Module" is selected (configured)

Photoreactor: 20mL quartz reaction tube (micro, small tube diameter, thick wall, 100% light-transmitting quartz reaction tube)

Irradiation Method: Zero-distance bottom irradiation

Light Source Type: Monochromatic LED light-emitting chip (customizable fixed wavelength as needed, non-traditional filter mode)

Light Source Power: 1-10W/site (adjustable power, COM-LED process, synchronous irradiation light source)

Light Source Cooling: Can be connected to external circulation cooling

Light Source Switching: Wavelength can be manually changed

Light Source Leakage: Minimal (total reflection, zero light pollution, high utilization rate)

Light Source Lifespan: 5000 hours (ensure cooling, prevent overheating)

Monochromatic Visible Light Source Coverage: 400-700nm (fully ensures consistency of experimental conditions, please refer to the light source type list for details)

Photochemical Reaction Channels: 10 (standard with 10 white lights)

White Light Source Description: Daylight color

Stirring Parameters: Standard "Stirring Heating"

Stirring Method: Synchronous surrounding magnetic stirring (equipped with German IKA stirring module)

Stirring Speed: 0-1500rpm (requires corresponding stirrer)

Stirring Bar One: Yes (Olive type*L13.5mm*220℃)

Material Addition Parameters:

Suitable Materials and Viscosity: Low viscosity liquids or dispersible solids

Anhydrous and Oxygen-Free Liquid Feeding: Yes (Syringe puncture injection)

Anhydrous and Oxygen-Free Solid Feeding: Yes (Zero-loss micro-injection under nitrogen flow protection or nitrogen flow-protected weighing dish placement)

Portable Glove Box Feeding: Yes (Reaction tube can be entirely placed into the glove box)

Anhydrous and Oxygen-Free Sample Collection: Yes (Online minimally invasive sampling)

Puncture Sealing Plug: Yes (Clean sealing plug can be repeatedly punctured, reusable, environmentally friendly and economical)

Secondary Sealing Function: Yes (Unique sealing plug puncture needle hole sealing, ensures airtightness of the sealed tube)

Schlenk Technical Parameters:

Reactor Sealing Method: O-ring threaded soft sealing

Extended Gas Line Quick Connection: Yes (New design for quick installation and double shut-off, arbitrary operation)

Schlenk Operation Panel: Yes (Simple and easy-to-use modular gas replacement platform)

Micro Positive Pressure Schlenk Line: Yes (Simulates glove box positive pressure system, equipped with high-quality storage气囊)

Reaction Gas Schlenk Line: Yes (Arbitrary switching between inert gas and reaction gas)

Inert Gas Schlenk Line: Yes (Arbitrary switching between inert gas and reaction gas)

Reaction Gas Supply Method: Cylinder supply (requires self-provided cylinder and pressure reducer)

Inert Gas Supply Method: Cylinder or fume hood supply (requires self-provided cylinder and pressure reducer)

Safety-Related Parameters:

Visual Protective Cover: Yes (Safety protection, resistant to environmental interference)

Safety Anti-Explosion Function: Yes (Safety protective cover)

Withstand Positive Pressure: ≤4atm (Maximum pressure tolerance for sealed tube reaction)

Overheat Protection: Yes (50-360℃任意设置, automatically cuts off power when temperature exceeds set value)

Other Feature Parameters:

Quick Hover Function: Yes (Quickly stop reaction, lift to stop)

Instrument Weather Resistance: Silver corrosion-resistant aluminum alloy shell (Aesthetically pleasing, corrosion-resistant protection)

Timing Function: Yes (Countdown for temperature control and stirring from 0-99h)

Weight and Volume: 22kg/D*W*H=45*35*65cm

Protection Level: Ip42

Power Supply: 650W, Ac220-240V, 50/60HZ

Operating Environment: Ambient temperature: 0～35℃, Relative humidity: 80%

Noise Level: 70dB

Complete Synthesis Accessories: Yes